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anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP"Stmivolatfte Oqpww'ct - Method EPA/CLP
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2J» fffetftwtf-Cfyife d b n n f t p f t r iampttfs) nctfved on November 9, 1993 wenand serrdvolta^oryvtksmd lead. Specific methods emptoyed jar the
QuaBty <asttr&tce/quaUfy contort (QA/QQ measures are employed to insure the qualityand dffietfoxcwacy of analytical data.$*f ^ •I*' r i F W f f * * B r * f c O
Oil antes Analyses (Votottie and SemtwIatKe)Instrument calibration - Instrument calibration 1s perfonwtd in accordance iwtt EPAcontract laboratory protocols. Instrument recatibfatfan is performed every 22 hows,Blank analysis - Method blanks an anatynxl at tho frequency specified by CLPprotocols. Method blanks demonstrate ifte level of background (laboratory)contamination. Blank data an presented on the results page along with the samptrdata*Surrogate spike anatysb - Each sample is fortified with recovery (surrogate) standardsprior to extraction or purging. The rtmv^ of the surro^e standards k a measure ofthe efficiency oftlte arudysb. A summary of surrogate recovery data, ft presented in theQA/QC Summary.Matrix spike/duplicate spike/blank spike • Sptcifa enafytes an added to selectedsamples prior to extraction crpuqfng. The results of ft* matrix spike/duplicate spikeanalyses an a measure of the precision and accuracy oftht analysis. The blank spttej provides method performance data in the absence of matrix effects. Spike duty areI included in the QA/QC Summary.
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