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Page 1: •J^Btfftt^H^rfOIrfAi b/f/t h-NOU-1&-199i 3 IS: TFRO 1M ^> TO WWC p.aa anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP "Stmivolatfte Oqpww'ct - Method EPA/CLP fiuali v AssurOHf^/Oudlitv

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Page 2: •J^Btfftt^H^rfOIrfAi b/f/t h-NOU-1&-199i 3 IS: TFRO 1M ^> TO WWC p.aa anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP "Stmivolatfte Oqpww'ct - Method EPA/CLP fiuali v AssurOHf^/Oudlitv

NOU-1&-1993 IS:iT 1 ^>

FROM TO WWC p.aa

anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP"Stmivolatfte Oqpww'ct - Method EPA/CLP

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2J» fffetftwtf-Cfyife d b n n f t p f t r iampttfs) nctfved on November 9, 1993 wenand serrdvolta^oryvtksmd lead. Specific methods emptoyed jar the

QuaBty <asttr&tce/quaUfy contort (QA/QQ measures are employed to insure the qualityand dffietfoxcwacy of analytical data.$*f ^ •I*' r i F W f f * * B r * f c O

Oil antes Analyses (Votottie and SemtwIatKe)Instrument calibration - Instrument calibration 1s perfonwtd in accordance iwtt EPAcontract laboratory protocols. Instrument recatibfatfan is performed every 22 hows,Blank analysis - Method blanks an anatynxl at tho frequency specified by CLPprotocols. Method blanks demonstrate ifte level of background (laboratory)contamination. Blank data an presented on the results page along with the samptrdata*Surrogate spike anatysb - Each sample is fortified with recovery (surrogate) standardsprior to extraction or purging. The rtmv^ of the surro^e standards k a measure ofthe efficiency oftlte arudysb. A summary of surrogate recovery data, ft presented in theQA/QC Summary.Matrix spike/duplicate spike/blank spike • Sptcifa enafytes an added to selectedsamples prior to extraction crpuqfng. The results of ft* matrix spike/duplicate spikeanalyses an a measure of the precision and accuracy oftht analysis. The blank spttej provides method performance data in the absence of matrix effects. Spike duty areI included in the QA/QC Summary.

1

Page 3: •J^Btfftt^H^rfOIrfAi b/f/t h-NOU-1&-199i 3 IS: TFRO 1M ^> TO WWC p.aa anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP "Stmivolatfte Oqpww'ct - Method EPA/CLP fiuali v AssurOHf^/Oudlitv

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Recaiwd:l: 11/11/93t: 11/12/93P*xc«nfe Moiatuea: HA.

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Page 7: •J^Btfftt^H^rfOIrfAi b/f/t h-NOU-1&-199i 3 IS: TFRO 1M ^> TO WWC p.aa anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP "Stmivolatfte Oqpww'ct - Method EPA/CLP fiuali v AssurOHf^/Oudlitv

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Page 8: •J^Btfftt^H^rfOIrfAi b/f/t h-NOU-1&-199i 3 IS: TFRO 1M ^> TO WWC p.aa anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP "Stmivolatfte Oqpww'ct - Method EPA/CLP fiuali v AssurOHf^/Oudlitv

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Page 9: •J^Btfftt^H^rfOIrfAi b/f/t h-NOU-1&-199i 3 IS: TFRO 1M ^> TO WWC p.aa anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP "Stmivolatfte Oqpww'ct - Method EPA/CLP fiuali v AssurOHf^/Oudlitv

A * . ;n o 1 *=i : JL o -tr' IWL w c: c J3 R.NBJ-1S-1993 17:03 FRC3W TO VMC

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Page 12: •J^Btfftt^H^rfOIrfAi b/f/t h-NOU-1&-199i 3 IS: TFRO 1M ^> TO WWC p.aa anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP "Stmivolatfte Oqpww'ct - Method EPA/CLP fiuali v AssurOHf^/Oudlitv

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Page 13: •J^Btfftt^H^rfOIrfAi b/f/t h-NOU-1&-199i 3 IS: TFRO 1M ^> TO WWC p.aa anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP "Stmivolatfte Oqpww'ct - Method EPA/CLP fiuali v AssurOHf^/Oudlitv

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Page 14: •J^Btfftt^H^rfOIrfAi b/f/t h-NOU-1&-199i 3 IS: TFRO 1M ^> TO WWC p.aa anpfyi E* an Indicated.-VolatBs Qrgantu - Method EPA/CLP "Stmivolatfte Oqpww'ct - Method EPA/CLP fiuali v AssurOHf^/Oudlitv

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