Act Age o Technica 2007
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R E S E A R C H P A P E R
Thermal conductivity measurements of road constructionmaterials in frozen and unfrozen state
Norbert I. Komle Hui Bing Wen Jie Feng Roman Wawrzaszek Erika S. Hu tter Ping He Wojciech Marczewski Borys Dabrowski Kathrin Schroer Tilman Spohn
Received: 5 January 2007 / Accepted: 16 May 2007 / Published online: 11 July 2007
Springer-Verlag 2007
Abstract A series of thermal conductivity measurements
for various materials was performed in a large climatechamber. The size of the chamber allowed the preparation
of relatively large samples in a controlled thermal envi-
ronment. Three types of thermal sensors were used: (1) two
needle probes; (2) a grid of temperature sensors, evenly
distributed inside the sample; (3) two additional thermal
probes, which were simplified versions of an instrument
originally developed for measuring thermal properties of
the ice/dust mixture expected to exist at the surface of a
comet nucleus. They consist of a series of individual
temperature sensors integrated into a glass fibre rod. Each
of these sensors can be operated in an active (heated) or
passive (only temperature sensing) mode. The following
sample materials were used: fine-grained reddish sand,
coarse-grained moist sand, gravels with various grain size
distributions from < 1 cm up to about 6 cm, and for
comparison and calibration pure water (with convection
suppressed by adding agar-agar), compact ice, and compactgranite. Of particular interest are the measurements with
composite samples, like stones embedded in an agar-agar
matrix. We describe the evaluation methods and present
the results of the thermal conductivity measurements.
Keywords Gravel Permafrost Sand Thermalconductivity
1 Introduction
The experiments reported in this paper served a twofold
purpose. First, in many physical and engineering problems
the thermal conductivity of the materials is a key parameter
controlling to a high extent the thermo-physical behaviour
of the system. For example, in the construction of road and
railway routes the distribution of artificially or naturally
generated heat in the underground determines the stability
of the bed and thus the safety of pathways. This is partic-
ularly important on seasonally or permanently frozen
ground, like the areas transected by the Qinghai-Tibet
Railway [14, 15].
The second aspect of our paper deals with the devel-
opment of suitable sensors for thermal conductivity mea-
surements itself. For our measurements we have used,
among else, so-called needle probes. They belong to the
category of transient or non steady state measurement
techniques. In general, when using a transient measurement
procedure, an unsteady temperature gradient is induced
inside the sample by a constant heat source. The heating
occurs over an adequate time period. The thermal con-
ductivity and/or diffusivity can be derived from the mea-
sured temperature response due to heating. Common
Presented at the 1st Asian Conference on Permafrost (ACOP),
Lanzhou, Gansu, China, 79 August 2006
N. I. Komle (&) E. S. HutterSpace Research Institute, Austrian Academy of Sciences,
Schmiedlstrasse 6, 8042 Graz, Austria
e-mail: norbert.koemle@oeaw.ac.at
H. Bing W. J. Feng P. HeCold and Arid Regions Environmental and Engineering
Research Institute (CAREERI), Chinese Academy of Sciences,
Lanzhou, China
R. Wawrzaszek W. Marczewski B. DabrowskiSpace Research Centre (SRC), Polish Academy of Sciences,
Warsaw, Poland
K. Schroer T. SpohnInstitut fur Planetologie (IFP), Universitat Munster,
Munster, Germany
123
Acta Geotechnica (2007) 2:127138
DOI 10.1007/s11440-007-0032-1
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commercialized techniques using this principle are needle
probes, hot wire methods, and the hot strip method. A
comprehensive summary of available transient as well as
steady state methods can be found, e.g. on the evitherm
website [5]. The advantages of transient measurement
techniques as compared to steady state techniques (like the
hot plate method) are (1) shorter measurement periods, (2)
suitability for a wide range of materials (solid and granular)and (3) a lower technical complexity. The latter property
makes them more suitable for field applications or even
application in space missions. On the other hand, the
measurement accuracy of transient methods is usually
lower than that of steady state methods. Therefore, steady
state methods may be more useful for calibration purposes.
Interpretation of needle probe measurements in terms of
thermal conductivity is most simple if the sample to be
measured has a homogeneous structure, is originally iso-
thermal, and is large enough that boundary effects can be
excluded. However, under more complex conditions,
which frequently occur in the natural environment, evalu-ation of thermal conductivity from measured temperature
data needs great care. We will consider an appropriate
reduction method for the raw data in order to derive reli-
able conductivity values from measured raw data.
Another way to evaluate thermal conductivity of a
medium indirectly is to use a grid of temperature sensors,
e.g. RTDs1 distributed across the sample and to introduce a
vertical temperature gradient. One way to achieve this is to
bring the bottom side of the sample in thermal contact with
a cooling plate. In our tests, such a method was used to
compliment and cross-check the needle probe measure-
ments.
In many applications the variation of thermal properties
with depth is of interest. This cannot be easily achieved by
standard needle probes like the Hukseflux TP02 [7]. They
can only provide average values over the length of the
probe. However, a thermal probe developed in the recent
years in the frame of ESAs2 comet mission Rosetta has
some ability to measure the variation of thermal properties
with depth in a soil. This instrument (MUPUS3), being a
part of the payload of the Rosetta Lander Philae, is cur-
rently on the way to its target comet Churyumov-Gera-
simenko. After landing on the comet nucleus surface, the
thermal properties of the cometary near-surface ice will be
derived [1, 8]. The probe consists of several segments
which can be separately heated in order to measure the
thermal properties of different layers subsequently. The
concept of MUPUS may also be useful for applications in
terrestrial environments. Therefore several probes of a
simplified variant named EXTASE4 have been built in the
frame of another project [10, 13]. First tests showed that
the interpretation of temperature data recorded by the
EXTASE probe in terms of thermal conductivity is by no
means an easy task. It demands a rather detailed thermal
model of the sensor itself and calibration measurements in
various well-known materials. In order to support this goaland to provide a broader basis for the interpretation of the
expected MUPUS measurements at the comet surface, we
have done some parallel tests with the EXTASE probes and
the needle probes in a well-known medium and compared
the results in terms of the obtained thermal conductivity
values.
2 Experimental equipment and setup
2.1 Climate chamber and sample container
The tests were performed in a thermally controlled envi-
ronment, namely a climate chamber of the CAREERI
(Lanzhou, China). This climate chamber allowed to
establish a homogeneous temperature environment in the
range of 40C to + 70C. The interior size of the chamber
is approximately a cube of 90 cm side length. A system of
fans permits fast relaxation of temperature inside the
chamber to a prescribed value. Furthermore, air humidity
inside the chamber can be controlled externally and set to a
prescribed value. During operation, the power devices of
the chamber are cooled by a cold water circuit.
The second major device used in our experiments is the
sample container. It is of rectangular shape (70 cm
70 cm 35 cm) and its sides are thermally insulated. The
bottom is connected to a cooling system working with
alcohol as cooling agent. This setup allows us to establish a
constant temperature at the bottom of the sample container,
which may differ from the set chamber temperature. Thus,
it can be used to establish a vertical temperature gradient
inside a test sample.
2.2 Thermal conductivity sensors
Three different methods for determining thermal conduc-
tivity were applied: (1) A commercial needle probe (Hu-
kseflux TP02); (2) a grid of individual temperature sensors
(platinum RTDs) which measures the temperature varia-
tions inside the sample during cooling periods; (3) a cus-
tom-built sequentially working probe (EXTASE) for1 Resistance Temperature Device, see http://www.temperature-
world.com/rtd.htm2 European Space Agency3 MUlti-PUrpose Sensors for surface and sub-surface science
4 EXperimental Thermal probe for Applications in Snow research and
Earth sciences
128 Acta Geotechnica (2007) 2:127138
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